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1 article(s) from Saitzek, Sébastien

Particle size effect in the mechanically assisted synthesis of β-cyclodextrin mesitylene sulfonate

Stéphane Menuel,
Sébastien Saitzek,
Eric Monflier and
Frédéric Hapiot

Beilstein J. Org. Chem. 2020, 16, 2598–2606, doi:10.3762/bjoc.16.211

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Scheme 1: The mechanically assisted synthesis of mono- and poly-β-CD mesitylene sulfonate (β-CDMts).

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Figure 1: SEM images of β-CD particles a) before grinding and ground for b) 5 min, c) 10 min, d) 29 min, e) 8...

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Figure 2: Granulometric composition of β-CD particles against time after grinding at 30 Hz.

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Figure 3: XRD patterns of β-CD powders obtained after different grinding times.

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Figure 4: Compared conversions of β-CD in the synthesis of β-CDMts.

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Figure 5: Variation of the mono/poly-substituted β-CDMts ratio with time. Reactions were done using untreated...

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Figure 6: Compared conversions of β-CD in the synthesis of β-CDMts in the presence of KOH (stoichiometric pro...

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Figure 7: Variation of the mono/poly-substituted β-CDMts ratio with time in the presence of KOH (stoichiometr...

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Published 22 Oct 2020

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